This review provides a comprehensive overview of the synthesis process of nanoscale materials and highlights key characterization methods used for nanomaterials and biomaterials. It emphasizes the importance of effective techniques for investigating materials at the nanoscale, as these are too small for the human eye to detect. The review also explores various approaches to producing nanoscale materials and offers insights into the application, development, advantages, and limitations of different experimental methods for nanoparticle characterization. A particular focus is placed on advanced characterization techniques and their role in data interpretation, aiming to guide novice researchers in the field of nanoscience and nanotechnology.
